한빛사 논문
Abstract
Jae-Min Kima, Seung-Hyun Choia, Gi-Hae Shina, Jin-Ha Leea, Seong-Ran Kangb, Kyun-Young Leec, Ho-Soo Limc, Tae Seok Kangc, Ok-Hwan Leea,*
a Department of Food Science and Biotechnology, Kangwon National University, Chuncheon 24341, Republic of Korea
b S-Food Guardians Co. Ltd, Seoul 02841, Republic of Korea
c Food Additives and Packages Division, Ministry of Food and Drug Safety, Osong Health Technology Administration Complex, 187 Osong, Chungcheongbuk-do 28159, Republic of Korea
*Corresponding author
Abstract
This study investigated a method for the validation and determination of measurement uncertainty for the simultaneous determination of synthetic phenolic antioxidants (SPAs) such as propyl gallate (PG), octyl gallate (OG), dodecyl gallate (DG), 2,4,5-trihydroxy butyrophenone (THBP), tert-butylhydroquinone (TBHQ), butylated hydroxyanisole (BHA), and butylated hydroxytoluene (BHT) in edible oils commonly consumed in Korea. The validated method was able to extract SPA residues under the optimized HPLC-UV and LC-MS/MS conditions. Furthermore, the measurement of uncertainty was evaluated based on the precision study. For HPLC-UV analysis, the recoveries of SPAs ranged from 91.4% to 115.9% with relative standard deviations between 0.3% and 11.4%. In addition, the expanded uncertainties of the SPAs ranged from 0.15 to 5.91. These results indicate that the validated method is appropriate for the extraction and determination of SPAs and can be used to verify the safety of edible oil products containing SPAs residues.
Keywords : Synthetic phenolic antioxidants (SPAs); Edible oils; Method validation; Measurement uncertainty; HPLC
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